Free PDF Crystal Structure Determination, by Werner Massa
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Crystal Structure Determination, by Werner Massa
Free PDF Crystal Structure Determination, by Werner Massa
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This textbook gives a concise introduction to modern crystal structure determination, emphasising both its theoretical background and the way it is actually carried out. The theoretical sections are supported by many illustrations, and lay emphasis on a good understanding rather than rigorous mathematics. The most important data collection techniques, and the methods of data reduction, structure solution and refinement are discussed from a practical point of view. Many tips and insights help readers to recognise and avoid possible errors and traps, and to judge the quality of results. The second edition has been considerably updated, especially the chapter on experimental methods, which is now mainly concerned with modern data collection using area-detectors.
- Sales Rank: #905350 in Books
- Brand: Brand:
- Published on: 2011-11-30
- Original language: English
- Number of items: 1
- Dimensions: 9.21" h x .56" w x 6.14" l, 1.05 pounds
- Binding: Hardcover
- 212 pages
- Used Book in Good Condition
Review
From the reviews:
"Distinguished by its attention to the practicalities of working with real crystals…a lucid and relatively concise account of modern crystal structure solution …valuable to anyone who has an interest in crystal structure refinement." The Geological Journal
"The book provides a nice balance between describing the mathematical fundamentals and offering practical advice on how to solve a crystal structure… appropriate for an undergraduate audience (particularly in chemistry) and for graduate students or researchers who find they need a better grasp of the subject… a very helpful addition to the collection of introductory texts in X-ray crystallography. Especially for its treatment of common errors in the collection of intensity data and in the interpretation of results."
Acta Crystallographica
"Details at great length the inherent pitfalls and errors that one may encounter when calculating crystal structures using new software programs. The author does an excellent job of describing these errors and ways to recognize them when they appear in your calculations." Mineralium Deposita
From the reviews of the second edition:
"This textbook gives a concise introduction to modern crystal structure determination … . The theoretical sections are supported by many illustrations, and lay emphasis on a good understanding … . The most important data collection techniques … are discussed from a practical point of view. Many tips and insights help readers to recognise and avoid possible errors and traps, and to judge the quality of results." (Chimie Nouvelle Societe Royale de Chimie, Vol. 23 (89), juin, 2005)
“‘Crystal Structure Determination’ gives a concise introduction to the subject, with particular emphasis placed on the manner in which contemporary analysis actually occurs. … The strengths of this book are numerous. The presentation is excellent: the diagrams are plentiful and often impressive, and the formatting of the text is very pleasing to the eye. … the research chemist with a desire to appreciate more fully a technique that they are likely to use with increasing frequency – the book should be a helpful companion.” (Andrew Bond, Crystallography News, June, 2004)
Most helpful customer reviews
7 of 7 people found the following review helpful.
The Book Doctors Recommend Most
By Dr. Peter Muller
This is the ideal book for the beginner and in my opinion a must-read. In the excellent translation by Robert O. Gould, "Crystal Structure Determination" by Werner Massa explains all the basics from symmetry in real and reciprocal space, over generation of X-rays and other practical aspects, all the way to structure solution and refinement. Massa keeps the book simple and understandable and uses mathematical formulae carefully and only when helpful or necessary.
I learned the basics of crystallography from the German original of "the Massa". Now that I am a teacher of crystallography myself, this is the book I recommend to my students.
0 of 0 people found the following review helpful.
excellent reference book
By Yoshi
I found this book good for reference or to review concepts in crystallography. You need at least to have previous knowledge in the basic concepts to understand it. The book goes right to the point, explanations are short but clear. It is an excellent summary of the theoretical details to remember when solving an structure.
0 of 0 people found the following review helpful.
Library book worth buying for keeps
By I. Young
I am currently using the library's copy of this text and am buying it since it has been such a good resource. The chapters are in evening-sized portions, it's highly readable, and while there are pieces I would organize differently, sections are presented in an order that flows and makes good sense. Some information about the instrumentation may be out of date (not the theory behind it, of course, but details of its execution) and this is worth keeping in mind. I tend to read this text as my first dive into any topic and supplement with multiple other resources. My class also uses Stout and Jensen for assigned readings and I also go online and pull up all sorts of diagrams, tables, PDFs and powerpoints that give me a better understanding of, for example, the Ewald construction than Massa's very short description gave me. In other words, Massa's text is a really excellent way to get comfortable with a topic, but it must be supplemented. I do find it easier to read the same chapters of other texts after getting an introduction from Massa, and for me, at least, that acclimation process saves a lot of time.
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